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Beilstein J. Org. Chem. 2008, 4, No. 24, doi:10.3762/bjoc.4.24
Graphical Abstract
Scheme 1: (a) (i) Br2/AcOH, (ii) CH2N2, (iii) separation by crystallization, (b) Zn/AcOH/RT (c) LiBr/DMF. The...
Figure 1: Reversed-phase HPLC analysis. Conditions: C18-column 8 mm x 10 cm, mobile phase 6:1 methanol/water ...
Figure 2: Scanning electron micrographs of the dried gels of compound 3 in mesitylene (a, inset: inverted via...
Figure 3: X-ray structure of arjuna-bromolactone 3. The length of the molecule (3O•••30C) is 1.26 nm.
Figure 4: Crystal packing diagram of arjuna-bromolactone 3. A network of hydrogen bridges leading to the form...